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- The
sample bottle number should ALWAYS match the rosette bottle number
– check and double-check this during the sample drawing
process. If you ever have any doubt about the sample, dump it
and start over.
- The sample bottles are stored inverted –
they should not be turned over until the sample has been
taken. If you need to step away from sampling for any reason
and have not filled the sample bottle, return it to the case inverted.
-
The bottles should never be stored empty so as
the old sample is dumped, use it to rinse any salt that may have
crystallized on the threads, thimble, and cap.
- Salt samples are usually drawn from the bottom
valve. Fill the bottle with ~40mls of seawater, cap loosely,
shake then dump, rinsing the threads and thimble. Repeat
– you should rinse the bottle 3 times; the dumping of old
sample does not count as a rinse.
- The last fill should be done without interruption
until overflowing, filling the bottle completely; pour ~10ml out over
the thimble, place it firmly in the bottle and cap. The caps
are brittle and should be tightened gently. If they crack,
retrieve a replacement from the spares Ziploc, keeping the thimble in
place. See photo for optimal fill height.
- Salts are taken from all closed rosette bottles
unless directed otherwise.
- Sample bottles are fragile – carefully
place them back in the correct slot. If you drop one on deck
or into the case and crack the glass, replace the cracked bottle from
the spares case, adding the bottle number. Redraw the sample.
- Once all the salts are taken:

- fill out a sample label (on the sample log
clipboard) with the time, your initials, total number of samples Place
the label in a plastic sleeve and into the box of samples
- take into the lab, adding it to the end
of the “salt box queue”; bring out an empty case
for next station.
- add your initials to the bottom of the sample
log’s salt column.
Common mistakes
are duplicate draws; samples returned to the case out of sequence
(common when more than one person is drawing salts); missing thimble
insert; not enough air (can crack the bottle as it warms and not allow
the analyst to load the sample); too much air (can shift the salinity
value or not give the analyst enough sample to measure); and cracked or
broken bottles (drops).
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